Antimony-121 Mossbauer spectroscopy study of vanadium antimonate prepared by mechanical milling

Berry, F.; Thomas, M. and Ren, X. (2005). Antimony-121 Mossbauer spectroscopy study of vanadium antimonate prepared by mechanical milling. In: Gracia, M.; Marco, J.F. and Plazaola, F. eds. Industrial Applications of the Mössbauer Effect · International Conference on the Industrial Applications of the Mössbauer Effect. AIP Conference Proceedings, 765. USA: American Institute of Physics/Springer, pp. 23–25.

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Abstract

Vanadium antimonate ,VSbO4, has been made by mechanical milling techniques.The material has a significantly smaller particle size ,ca 23nm,compared with vanadium antimonate prepared by conventional calcination methods.Antimony-121 Mossbauer spectroscopy shows antimony to be present as Sb5+.

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