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A carbon nano tube electron impact ionisation source for low-power, compact spacecraft mass spectrometers

Sheridan, Simon; Bardwell, Max; Morse, Andrew and Morgan, Geraint (2012). A carbon nano tube electron impact ionisation source for low-power, compact spacecraft mass spectrometers. Advances in Space Research, 49(8) 1245 -1252.

DOI (Digital Object Identifier) Link: http://dx.doi.org/10.1016/j.asr.2012.01.018
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Abstract

A novel ionisation source which uses commercially available Carbon Nano Tube devices is demonstrated as a replacement for a filament based ionisation source in an ion trap mass spectrometer. The carbon nanotube ion source electron emission was characterised and exhibited typical emission of 30 ± 1.7 µA with an applied voltage differential of 300 V between the carbon nanotube tips and the extraction grid. The ion source was tested for longevity and operated under a condition of continuous emission for a period of 44 hours; there was an observed reduction in emission current of 26.5% during operation. Spectra were generated by installing the ion source into a Finnigan Mat ITD700 ion trap mass spectrometer; the spectra recorded showed all of the characteristic m/z peaks from m/z 69 to m/z 219. Perfluorotributylamine spectra were collected and averaged contiguously for a period of 48 hours with no significant signal loss or peak mass allocation shift. The low power requirements and low mass of this novel ionisation source are considered be of great value to future space missions where mass spectrometric technology will be employed.

Item Type: Journal Article
Copyright Holders: 2012 Committee on Space Research
ISSN: 0273-1177
Project Funding Details:
Funded Project NameProject IDFunding Body
Not SetNot SetSTFC (Science & Technology Facilities Council)
Academic Unit/Department: Science > Physical Sciences
Interdisciplinary Research Centre: Centre for Earth, Planetary, Space and Astronomical Research (CEPSAR)
Item ID: 31681
Depositing User: Simon Sheridan
Date Deposited: 31 Jan 2012 11:23
Last Modified: 21 Nov 2013 09:50
URI: http://oro.open.ac.uk/id/eprint/31681
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