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Using pulsed neutron transmission for crystalline phase imaging and analysis

Steuwer, A.; Withers, P. J.; Santisteban, J. R. and Edwards, L. (2005). Using pulsed neutron transmission for crystalline phase imaging and analysis. Journal of Applied Physics, 97(7), article no. 074903.

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DOI (Digital Object Identifier) Link: http://dx.doi.org/10.1063/1.1861144
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Abstract

The total scattering cross section of polycrystalline materials in the thermal neutron region contains valuable information about the scattering processes that neutrons undergo as they pass through the sample. In particular, it displays characteristic discontinuities or Bragg edges of selected families of lattice planes. We have developed a pixelated time-of-flight transmission detector able to record these features and in this paper we examine the potential for quantitative phase analysis and crystalline phase imaging through the examination of a simple two-phase test object. Two strategies for evaluation of the absolute phase volumes (path lengths) are examined. The first approach is based on the evaluation of the Bragg edge amplitude using basic profile information. The second approach focuses on the information content of certain regions of the spectrum using a Rietveld-type fit after first identifying the phases via the characteristic edges. The phase distribution is determined and the coarse chemical species radiographic image reconstructed. The accuracy of this method is assessed.

Item Type: Journal Article
Copyright Holders: 2005 American Institute of Physics
ISSN: 0021-8979
Project Funding Details:
Funded Project NameProject IDFunding Body
Not SetGR/L62801EPSRC (Engineering and Physical Sciences Research Council)
Not SetGR/L62498EPSRC (Engineering and Physical Sciences Research Council)
Extra Information: This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics.
Academic Unit/Department: Mathematics, Computing and Technology > Engineering & Innovation
Mathematics, Computing and Technology
Item ID: 18233
Depositing User: Colin Smith
Date Deposited: 14 Sep 2009 15:58
Last Modified: 26 Mar 2014 05:48
URI: http://oro.open.ac.uk/id/eprint/18233
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